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川源科技 ACCFILM 漿料電阻測試系統(tǒng)

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詳細介紹

在鋰離子電池生產制造中,將液體介質與正負極活性材料、導電劑、粘結劑混合均勻,得到電池漿料,然后涂布在集流體上,利用干燥烘烤等除去溶劑(水或NMP),毫無疑問作為鋰電池生產的第一道工序,勻漿配料是重中之重,是一切性能的基礎。


In the manufacture of lithium-ion battery production, with liquid medium is the positive and negative active materials, conductive agent, binder are mixed evenly to get the battery slurry, and then coated on the fluid collector, using drying and baking to remove the solvent (NMP) or water, there is no doubt that as the first step of lithium-ion battery production,homogenate ingredients are the most important and the basis of all performance.

而漿料的各項特性參數又是表征或衡量漿料的基礎,而漿料電導性又是決定電芯導電性的重要參數,所以找到一種測量漿料電導性及穩(wěn)定性的方法及儀器非常重要。


And the characteristic parameters of slurry is the basis of characterization or measurement of slurry, and the conductivity of slurry is an important parameter to determine the conductivity of the cell, so it is very important to find a method and instrument to measure the conductivity and stability of slurry.



5402208acad941f961010bdc782dd4c.png 漿料電阻測量在漿料快速評估、品質監(jiān)控等過程中發(fā)揮以下作用:

Measurement of slurry resistance plays the following roles in the process of slurry rapid evaluation and quality monitoring:

18e797313825510879627f80d227ca6.png

1. 綜合評估不同攪拌工藝對膠料電導率(包括分散性、沉降等)影響;


The influence of different stirring processes on the conductivity (including dispersion settlement, etc.) of the compound was comprehensively evaluated

2. 針對生產過程中漿料批次穩(wěn)定性的評估;


Evaluation of batch stability of slurry during production

3. 針對不同配方漿料導電性評估;


Conductivity evaluation of different slurry formulations;




5402208acad941f961010bdc782dd4c.png 漿料電導率測量原理

Principle of slurry conductivity measurement

18e797313825510879627f80d227ca6.png

                                                               電阻率,Resistivity,QQ截圖20220208232234.jpg

測量方法:將準備的的漿料導入干凈的電極測試杯中(蓋過測試杯指示線)或直接將測試電極筆放入漿料量杯中,開啟軟件,選擇對應的測試模式,開始測試,數據將自動保存;


Measurement method: Put the prepared slurry into a clean electrode test cup (over the indicator line of the test cup) or directly put the test electrode pen into the slurry measuring cup, open the software, select the corresponding test mode, start the test, and the data will be automatically saved;

測量參數:電導率、電導率、穩(wěn)定系數、溫度、時間

Measurement parameters:   conductivity, stability coefficient, temperature, time



產品特色




5402208acad941f961010bdc782dd4c.png MSA可靠性分析

MSA reliability analysis

18e797313825510879627f80d227ca6.png

ACCFILM漿料電阻測試儀測試為可再現性測試,測試通過標準樣品進行測量可靠性分析;

ACCFILM slurry resistance tester test is reproducibility test, test through the standard sample measurement reliability analysis;



5402208acad941f961010bdc782dd4c.png 應用領域與范圍


Application field and scope

18e797313825510879627f80d227ca6.png

本測量系統(tǒng)適用于企業(yè)、高等院校、科研院所及分析檢測機構、是檢驗對電池及半導體材料的漿料電導率及其穩(wěn)定性進行測量,其主要輸出測量測試如下:


The measurement system is suitable for enterprises, universities, research institutes and analysis and testing institutions, is to test the battery and semiconductor material slurry conductivity and stability measurement, its main output measurement test is as follows:



5402208acad941f961010bdc782dd4c.png 輸出測量參數(VS.傳統(tǒng)四探針)

Output measurement parameters (vs. conventional four-probe)

18e797313825510879627f80d227ca6.png

序號

項目

漿料電阻測試系統(tǒng)

1

電導率conductivity


可以Yes


2

電導率與時間關系

The relationship between conductivity and time


可以Yes


3

電導率與溫度關系

     Conductivity and temperature relation


可以Yes


4

漿料穩(wěn)定系數

            Stability coefficient of slurry


可以Yes




5402208acad941f961010bdc782dd4c.png 行業(yè)應用情況

Industry Application

18e797313825510879627f80d227ca6.png

基于自營與合作的營銷及服務模式,ACCFILM系列產品自2016年完成S發(fā)后,已服務近100家客戶,在2020年實現為市場出貨前十的企業(yè)中其中7家提供產品服務, “ACCFILM”品牌已經成為新能源動力電池細分領域的代名詞。


Based on the marketing and service mode of self-operation and cooperation, ACCFILM series products had served nearly 100 customers since the global debut in 2016. In 2020, ACCFILM had provided products and services for 7 of the top 10 companies in the global market. "ACCFILM" brand had become synonymous with the new energy power battery segment.


5402208acad941f961010bdc782dd4c.png 應用案例

application case

18e797313825510879627f80d227ca6.png

1.負極漿料中應用的穩(wěn)定性評估


Stability evaluation for applications in negative slurry

不同CMC(漿料穩(wěn)定劑)應用于石墨負極配方中,將影響漿料的沉降性能(穩(wěn)定性),通過監(jiān)控漿料的電導率測量變化,可判定評價原材料的應用效果;

Different CMC (slurry stabilizer) applied to graphite anode formula will affect the settling property (stability) of slurry. The application effect of raw materials can be evaluated by monitoring the conductivity measurement changes of slurry.

應用:材料篩選評價、穩(wěn)定性監(jiān)控


Application: material screening evaluation, stability monitoring

漿料配方簡要說明:石墨95.3%,CMC2或CMC1 1.3%,SBR1.9%,SP 1.5%;


Formulation of slurry: graphite 95.3%, CMC2 or CMC1 1.3%, SBR1.9%,SP 1.5%;



2. 不同黏度(稀釋)漿料電阻率評估

Resistivity evaluation of slurry with different viscosity (dilution)

對于實驗應用案例1的漿料進行稀釋,稀釋前后漿料的電阻率明顯增大,導電性能降低,為后續(xù)漿料開發(fā)提供新的測量參數。

After diluting the slurry of experimental application case 1, the resistivity of the slurry increased significantly and the conductivity decreased, providing new measurement parameters for the subsequent slurry development.


                                  


3. 不同保存時間漿料電阻率評估

Resistivity evaluation of slurry with different storage time

對于負極漿料進行不同時間存儲后,與新鮮漿料對比,原漿料出現明顯的沉降(具體效果如圖3);對兩個漿料的電阻情況進行測試,具體結果如表:


For the negative slurry stored for different time, compared with the fresh slurry, the original slurry has obvious settlement (see Figure 3). The resistance of the two pastes was tested. The specific results are shown in the table:


4. 客戶提供數據案例

Customer provides data case

某客戶對于其某款漿料進行稀釋實驗的數據,其稀釋倍數與電導率成等比例線性關系;


A customer for its a slurry dilution test data, the dilution ratio and conductivity into equal proportion linear relationship;

具體結果如右圖數據曲線:


Specific results are shown in the data curve on the right:

5.不同固含量漿料電導率

Conductivity of slurry with different solid content

通過漿料電導率測試可實現特定配方的適合固含量的判定;

The determination of suitable solid content of a specific formula can be realized through the test of slurry conductivity.


5402208acad941f961010bdc782dd4c.png 系統(tǒng)參數

system parameter

18e797313825510879627f80d227ca6.png

系統(tǒng)型號

System Product Name


Skit C3

主要功能

      main function


電導率、溫度、漿料穩(wěn)定性監(jiān)控

性能

performance


電阻率量程

Resistivity range


2.00Ω·cm~100.0MΩ·cm

電導率量程

Conductivity range


0.01μS/cm~500mS/cm

精度

precision


±0.5%

最小分辨率

minimum resolution


0.01μS/cm

溫度

temperature


量程

range


0-40℃

精度

precision


±0.5℃

分辨率

resolution ratio


0.1℃

測量杯/測量筆

Measuring cup/measuring pen


多通道測量杯或單通道測量筆配置

Multi-channel measuring cup or single channel measuring pen configuration


安全防護

    safety protection


人體工程學安全防護設計

                         Ergonomic safety protection design


軟件功能

   software function


全自動通訊連接

                    Fully automatic communication connection


一鍵自動調零及校準

                   One button automatic zero and calibration


測量次數統(tǒng)計

                                     Measurement statistics


單點或線性測試模式可選

                     Single point or linear test mode is optional


生產測量輔助判定

                Production measurement auxiliary decision


實時數據采集記錄與預覽

                Real-time data acquisition record and preview


測試數據編輯等

                                   Test data editing, etc


機構尺寸(L*W*H)Mechanical Drawings


~300mm*185mm*150mm

電源

        power supply


220V,50Hz

重量

               weight


5kg




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